Change search
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf
The effect of microstructural features, defects and surface quality on the fatigue performance in Al-Si-Mg Cast alloys
Jönköping University, School of Engineering, JTH, Materials and Manufacturing.ORCID iD: 0000-0001-5753-4052
2023 (English)Doctoral thesis, comprehensive summary (Other academic)
Abstract [en]

Global warming is driving industry to manufacture lighter components to reduce carbon dioxide (CO2) emissions. Promising candidates for achieving this are aluminium-silicon (Al-Si) cast alloys, which offer a high weight-to-strength ratio, excellent corrosion resistance, and good castability. However, understanding variations in the mechanical properties of these alloys is crucial to producing high-performance parts for critical applications. Defects and oxides are the primary reasons cast components in fatigue applications are rejected, as they negatively impact mechanical properties.

A comprehensive understanding of the correlation between fatigue performance and parameters such as the α-aluminium matrix, Al-Si eutectic, surface roughness, porosities, hydrogen content, oxides, and intermetallic phases in Al-Si castings has not been reached.

The research presented in this thesis used state-of-the-art experimental techniques to investigate the mechanical properties and crack-initiation and propagation behaviour of Al-Si-Mg cast alloy under cyclic loading. In-situ cyclic testing was conducted using scanning electron microscopy (SEM) combined with electron back-scattered diffraction (EBSD), digital image correlation (DIC), and focused ion beam (FIB) milling. These techniques enabled a comprehensive study of parameters affecting fatigue performance, including hydrogen content, surface roughness, oxides, and intermetallic phases. More specifically, we investigated the effect of melt quality, copper (Cu) content, oxide bifilms, surface quality, and porosity.

The increased Cu concentration in heat-treated Al-Si alloys increased the amount of intermetallic phases, which affected the cracking behaviour. Furthermore, oxide bifilms were detected at crack-initiation sites, even in regions far away from the highly strained areas. Si- and Iron (Fe)-rich intermetallics were observed to have precipitated on these bifilms. Due to their very small size, these oxides are generally not detected by non-destructive inspections, but affect mechanical properties because they appear to open at relatively low tensile stresses. Finally, Al-Si alloy casting skins showed an interesting effect in terms of improving fatigue performance, highlighting the negative effect of surface polishing for such alloys.

Abstract [sv]

Klimatförändringar runt om i världen driver industrin att tillverka lättare komponenter för att minska utsläppen av koldioxid (CO2). Lovande kandidater för att uppnå detta är aluminium-silikon (Al-Si) gjutna legeringar, som erbjuder hög vikt-till-styrkeförhållande, utmärkt korrosionsbeständighet och god gjutbarhet. Förståelsen av variationer i de mekaniska egenskaperna hos dessa legeringar är dock avgörande för att producera högpresterande komponenter för kritiska tillämpningar. Defekter och oxider är de främsta orsakerna till att gjutna komponenter i utmattningsapplikation avvisas, eftersom de påverkar de mekaniska egenskaperna negativt.

En heltäckande förståelse av sambandet mellan mekaniska egenskaper och parametrar som mikrostrukturella faser, ytfinhet, porositet och oxider i Al-Si-gjutningar har ännu inte blivit fullständigt kartlagd.

Forskningen som presenteras i denna avhandling använde toppmoderna experimentella tekniker för att undersöka de mekaniska egenskaperna samt initiering och propagering av sprickor i Al-Si-Mg-gjutgods under utmattningstester. Dessa tekniker möjliggjorde en omfattande studie av parametrar som påverkar utmattningen, inklusive väteinnehåll, ytfinhet, oxider och intermetalliska faser.

Den ökade Cu-koncentrationen i värmebehandlade Al-Si-legeringar ökade mängden intermetalliska faser, vilket påverkade sprickbeteendet. Vidare upptäcktes oxidfilmer på platser där sprickor initierades, även i områden långt borta från de mest påverkade områdena Kisel och järnfaser observerades ha kärnbildat på dessa oxidfilmer. På grund av deras mycket små storlek upptäcks dessa oxider vanligtvis inte av icke-destruktiva inspektioner, men de påverkar mekaniska egenskaper eftersom de tycks öppna vid relativt låga dragspänningar. Slutligen visade gjutskinnet på Al-Si-komponenter en intressant effekt när det förbättrade utmattningsegenskaperna och belyser den negativa effekten av bearbetning på dessa komponenter.

Place, publisher, year, edition, pages
Jönköping: Jönköping University, School of Engineering , 2023. , p. 125
Series
JTH Dissertation Series ; 084
Keywords [en]
Aluminum-Silicon alloys, defects, material characterization, fatigue performance, digital image correlation
National Category
Metallurgy and Metallic Materials
Identifiers
URN: urn:nbn:se:hj:diva-62909ISBN: 978-91-89785-01-4 (print)ISBN: 978-91-89785-02-1 (electronic)OAI: oai:DiVA.org:hj-62909DiVA, id: diva2:1813756
Public defence
2023-12-15, E1405 (Gjuterisalen), School of Engineering, Jönköping, 10:00 (English)
Opponent
Supervisors
Note

Included in doctoral thesis in manuscript form.

Available from: 2023-11-21 Created: 2023-11-21 Last updated: 2025-10-13Bibliographically approved
List of papers
1. A simple procedure to assess the Complete Melt Quality in aluminium castings: implementation in a die-casting and a rheo-casting
Open this publication in new window or tab >>A simple procedure to assess the Complete Melt Quality in aluminium castings: implementation in a die-casting and a rheo-casting
2024 (English)In: International Journal of Cast Metals Research, ISSN 1364-0461, E-ISSN 1743-1336, Vol. 37, no 1, p. 71-79Article in journal (Refereed) Published
Abstract [en]

A new simple approach was developed to assess the Complete Melt Quality of aluminium cast alloys throughout the production line. The approach relies on the concurrent use of reduced pressure tests (RPT) and tensile tests at each station in the production line when the melt is transferred and/or processed. These tests can be used to determine the source of melt-related problems in the production line. Two case studies from the procedure of both an aluminium die-casting and a rheo-casting plant showed that melts were significantly damaged in the tower furnace and got progressively more damaged through the production line proven by the RPT, tensile test, and fracture surface analysis results.

Place, publisher, year, edition, pages
Taylor & Francis, 2024
Keywords
Melt transfers, bifilms, degassing, liquid metal damage, porosity
National Category
Metallurgy and Metallic Materials
Identifiers
urn:nbn:se:hj:diva-63218 (URN)10.1080/13640461.2023.2293415 (DOI)001125756600001 ()2-s2.0-85179712295 (Scopus ID);intsam;924887 (Local ID);intsam;924887 (Archive number);intsam;924887 (OAI)
Funder
VinnovaKnowledge Foundation
Available from: 2024-01-08 Created: 2024-01-08 Last updated: 2025-10-13Bibliographically approved
2. On the Effectiveness of Rotary Degassing of Recycled Al-Si Alloy Melts: The Effect on Melt Quality and Energy Consumption for Melt Preparation
Open this publication in new window or tab >>On the Effectiveness of Rotary Degassing of Recycled Al-Si Alloy Melts: The Effect on Melt Quality and Energy Consumption for Melt Preparation
Show others...
2023 (English)In: Sustainability, E-ISSN 2071-1050, Vol. 15, no 6, article id 5189Article in journal (Refereed) Published
Abstract [en]

The effectiveness of rotary degassing on the defect formation and mechanical properties of the final casting of aluminium alloy EN AC 46000 was investigated, along with its impact on the energy consumption in the casting furnace. In the melt preparation prior to casting, the molten metal is usually transported from the melting furnace to the casting furnace with rotary degassing as a cleaning procedure. Under the conditions of this specific study, negligible degradation was observed in the mechanical properties of the final cast component in an aluminium EN AC 46000 alloy after removing the rotary degassing step in the process. Furthermore, removing the rotary degassing step led to a reduced temperature drop in the melt, thus minimizing the need for reheating (energy consumption) by up to 75% in the casting furnace. The reduced energy consumption was up to 124,000 kWh in yearly production in a 1500 kg casting furnace. The environmental impact showed a similar to 1500 kg reduction in CO2 for one 1500 kg electrical casting furnace in a year.

Place, publisher, year, edition, pages
MDPI, 2023
Keywords
aluminium, sustainability, energy, casting, carbon footprint
National Category
Materials Engineering
Identifiers
urn:nbn:se:hj:diva-60220 (URN)10.3390/su15065189 (DOI)000960079100001 ()2-s2.0-85186230318 (Scopus ID)GOA;intsam;876312 (Local ID)GOA;intsam;876312 (Archive number)GOA;intsam;876312 (OAI)
Funder
Vinnova
Available from: 2023-04-21 Created: 2023-04-21 Last updated: 2025-10-13Bibliographically approved
3. The impact of HIP process and heat treatment on the fatigue performance of an Al-Si-Mg alloy component
Open this publication in new window or tab >>The impact of HIP process and heat treatment on the fatigue performance of an Al-Si-Mg alloy component
(English)Manuscript (preprint) (Other academic)
National Category
Metallurgy and Metallic Materials
Identifiers
urn:nbn:se:hj:diva-52086 (URN)
Note

Submitted to conference.

Available from: 2021-03-23 Created: 2021-03-23 Last updated: 2025-10-13
4. The influence of copper addition on crack initiation and propagation in an Al–Si–Mg alloy during cyclic testing
Open this publication in new window or tab >>The influence of copper addition on crack initiation and propagation in an Al–Si–Mg alloy during cyclic testing
Show others...
2020 (English)In: Materialia, E-ISSN 2589-1529, Vol. 12, article id 100787Article in journal (Refereed) Published
Abstract [en]

The effect of copper (Cu) addition up to 3.2 wt% on crack initiation and propagation in an Al–Si–Mg cast alloy was investigated using in-situ cyclic testing in the as-cast condition. A combination of digital image correlation, electron backscatter diffraction, and scanning electron microscopy was used to investigate crack initiation and propagation behaviour during in-situ cyclic testing. The results showed that Cu-rich intermetallic compounds with the addition of Cu up to 1.5 wt% do not affect the fatigue behaviour of these alloys, and that crack propagation in these cases is trans-granular and trans-dendritic. However, increasing the concentration of the Cu retained in the primary α-Al matrix in solid solution and Cu-containing precipitates delayed crack propagation during cyclic testing. The results showed that strain accumulation was highest at the grain boundaries; however, the crack preferred to propagate along or across primary α-Al dendrites due to the relatively lower mechanical strength of the matrix compared to the eutectic and intermetallic phases. Moreover, the addition of Cu of more than 3.0 wt% to Al-Si-Mg alloys changes the fatigue behaviour that a rapid failure occurs. 

Place, publisher, year, edition, pages
Elsevier, 2020
Keywords
Al alloys, Cu intermetallics, Cyclic loading, Digital image correlation, In situ, Aluminum alloys, Copper compounds, Crack initiation, Crack propagation, Cracks, Grain boundaries, Intermetallics, Magnesium alloys, Scanning electron microscopy, Silicon alloys, Ternary systems, Copper additions, Crack initiation and propagation, Digital image correlations, Effect of coppers, Electron back scatter diffraction, Fatigue behaviour, Intermetallic phasis, Strain accumulations, Fatigue of materials
National Category
Materials Engineering
Identifiers
urn:nbn:se:hj:diva-50104 (URN)10.1016/j.mtla.2020.100787 (DOI)000559334400003 ()2-s2.0-85086821863 (Scopus ID)HOA;intsam;1454593 (Local ID)HOA;intsam;1454593 (Archive number)HOA;intsam;1454593 (OAI)
Available from: 2020-07-17 Created: 2020-07-17 Last updated: 2025-10-13Bibliographically approved
5. The complex interaction between microstructural features and crack evolution during cyclic testing in heat-treated Al–Si–Mg–Cu cast alloys
Open this publication in new window or tab >>The complex interaction between microstructural features and crack evolution during cyclic testing in heat-treated Al–Si–Mg–Cu cast alloys
Show others...
2021 (English)In: Materials Science & Engineering: A, ISSN 0921-5093, E-ISSN 1873-4936, Vol. 825, article id 141930Article in journal (Refereed) Published
Abstract [en]

The study aimed to investigate crack initiation and propagation at the micro-scale in heat-treated Al–7Si–Mg cast alloys with different copper (Cu) contents. In-situ cyclic testing in a scanning electron microscope coupled with electron back-scattered diffraction and digital image correlation was used to evaluate the complex interaction between the crack path and the microstructural features. The three-nearest-neighbour distance of secondary particles was a new tool to describe the crack propagation in the alloys. The amount of Cu retained in the α-Al matrix after heat treatment increased with the Cu content in the alloy and enhanced the strength with a slight decrease in elongation. During cyclic testing, the two-dimensional (2D) crack path appeared with a mixed propagation, both trans- and inter-granular, regardless of the Cu content of the alloy. On fracture surfaces, multiple crack initiation points were detected along the thickness of the samples. The debonding of silicon (Si) particles took place during crack propagation in the Cu-free alloy, while cracking of Si particles and intermetallic phases occurred in the alloy with 3.2 wt% Cu. Three-dimensional tomography using focused ion beam revealed that the improved strength of the α-Al matrix changes the number of cracked particles ahead of the propagating crack with Cu concentration above 1.5 wt%.

Place, publisher, year, edition, pages
Elsevier, 2021
Keywords
Aluminium alloys, Casting methods, Characterisation, Electron microscopy, Fatigue, After-heat treatment, Aluminum alloys, Copper alloys, Crack initiation, Crack propagation, Cracks, Fatigue testing, Ion beams, Magnesium alloys, Scanning electron microscopy, Cast alloys, Casting method, Characterization, Crack paths, Cracks propagation, Cu content, Cyclic testing, matrix, Microstructural features, Silicon particles, Fatigue of materials
National Category
Materials Engineering
Identifiers
urn:nbn:se:hj:diva-54357 (URN)10.1016/j.msea.2021.141930 (DOI)000696737700001 ()2-s2.0-85113150418 (Scopus ID)HOA;intsam;761074 (Local ID)HOA;intsam;761074 (Archive number)HOA;intsam;761074 (OAI)
Note

Included in licentiate thesis in manuscript form.

Available from: 2021-08-30 Created: 2021-08-30 Last updated: 2025-10-13Bibliographically approved
6. Revealing and simulating the effect of hidden damage on local and full-field deformation behaviour of cast aluminium
Open this publication in new window or tab >>Revealing and simulating the effect of hidden damage on local and full-field deformation behaviour of cast aluminium
2023 (English)In: IOP Conference Series: Materials Science and Engineering, ISSN 1757-8981, E-ISSN 1757-899X, Vol. 1281, no 1, article id 012066Article in journal (Refereed) Published
Abstract [en]

Pores have been the main focus of quality assurance in castings. Latest research has shown that in aluminium castings pores can form only if there is existing entrainment damage, i.e., pores are merely the visible parts of the entrainment damage, and usually invisible damage is much more extensive. However, its effect on deformation behaviour has not been previously established or observed in-situ. This work applies 2D Digital Image Correlation (DIC) to an in-situ full-field stress-strain analysis of tensile samples with a non-conventional heterogeneous stress distribution. The observations reveal that the effect of hidden damage extends far beyond its impact on fracture behaviour and is responsible for initiating local strain concentrations during deformation. By extracting local stress-strain data, FE simulations have been performed to mimic the effect of local hidden damage on the heterogeneous stress-strain field. SEM and FIB-SEM analysis has been applied to investigate the cause for the strain concentrations. The combined results show that hidden damage in the form of oxide films is not only responsible for premature fracture, but also affects the deformation behaviour of tensile samples by introducing dispersed strain concentrations.

Place, publisher, year, edition, pages
Institute of Physics (IOP), 2023
National Category
Metallurgy and Metallic Materials
Identifiers
urn:nbn:se:hj:diva-62908 (URN)10.1088/1757-899x/1281/1/012066 (DOI)POA;intsam;62908 (Local ID)POA;intsam;62908 (Archive number)POA;intsam;62908 (OAI)
Conference
16th International Conference on Modelling of Casting, Welding and Advanced Solidification Processes (MCWASP 2023), 18-23 June 2023, Banff, Canada
Funder
Vinnova
Available from: 2023-11-21 Created: 2023-11-21 Last updated: 2025-10-13Bibliographically approved
7. On the secondary cracks during crack propagation in an Al-Si-Cu-Mg alloy: An in-situ study
Open this publication in new window or tab >>On the secondary cracks during crack propagation in an Al-Si-Cu-Mg alloy: An in-situ study
Show others...
2023 (English)In: Materials Characterization, ISSN 1044-5803, E-ISSN 1873-4189, Vol. 203, article id 113046Article in journal (Refereed) Published
Abstract [en]

During in situ cyclic testing of hot isostatically pressed and heat-treated Al-5Si-0.5 Mg-1Cu alloy castings, cracks were observed to open up in places far away from the area of stress concentration. Cyclic testing was interrupted to assess these cracks. Analysis showed that these cracks originated from oxide bifilms that were entrained in the liquid state. Moreover, Si and Fe-rich intermetallics were observed to have precipitated on these bifilms. These finding makes it necessary to re-evaluate how damage is interpreted in mechanical studies. Entrainment damage, which takes place in the liquid state, may remain invisible in non-destructive inspection and can significantly affect fatigue properties when bifilms open up under low tensile stresses and present the propagating crack a path of low resistance during propagation.

Place, publisher, year, edition, pages
Elsevier, 2023
Keywords
Al alloy, in-situ fatigue test, Bifilms, Entrainment damage, Oxides, Aluminum alloys, Copper alloys, Fatigue damage, Fatigue testing, Magnesium alloys, Nondestructive examination, Silicon alloys, Al-alloy, Alloy castings, Cracks propagation, Cyclic testing, In-Situ Study, Liquid state, Secondary cracks, Cracks
National Category
Materials Engineering
Identifiers
urn:nbn:se:hj:diva-61590 (URN)10.1016/j.matchar.2023.113046 (DOI)001028802300001 ()2-s2.0-85161632216 (Scopus ID)HOA;intsam;887741 (Local ID)HOA;intsam;887741 (Archive number)HOA;intsam;887741 (OAI)
Funder
Vinnova, 02943Knowledge Foundation, 20200219H
Available from: 2023-06-26 Created: 2023-06-26 Last updated: 2025-10-13Bibliographically approved
8. On the combined effects of surface quality and pore size on the fatigue life of Al–7Si–3Cu–Mg alloy castings
Open this publication in new window or tab >>On the combined effects of surface quality and pore size on the fatigue life of Al–7Si–3Cu–Mg alloy castings
Show others...
2023 (English)In: Materials Science & Engineering: A, ISSN 0921-5093, E-ISSN 1873-4936, Vol. 885, article id 145618Article in journal (Refereed) Published
Abstract [en]

This study has aimed to determine the effects of surface quality and pore size, obtained by different levels of hydrogen content of the liquid metal, on the fatigue behavior of an Al–7%Si–3%Cu–Mg casting alloy. Three surface conditions have been studied: as-cast rough, as-cast smooth, and standard machined and polished surface. The S–N curves have shown that surface roughness and hydrogen content individually impact fatigue strength. Surprisingly, the fatigue strength of machined and polished samples, which aligns with standard testing practices, is significantly reduced, compared to other conditions. Fatigue cracks have been observed to initiate at the pores just below the as-cast surface or on the machined surfaces. In all cases, pores have been observed to be surrounded by bifilms. Moreover, hydrogen content and roughness of the as-cast surface have been found to interact to determine the fatigue performance. These findings necessitate a re-evaluation of fatigue testing procedures for cast aluminum components.

Place, publisher, year, edition, pages
Elsevier, 2023
Keywords
Bifilms, Fracture, Oxide skin, Pores, Weibull, Fatigue testing, Hydrogen, Magnesium alloys, Surface properties, Surface roughness, As-cast, Cast surface, Combined effect, Fatigue strength, Hydrogen contents, Machined surface, Oxide skins, Pore, Pore size
National Category
Materials Engineering
Identifiers
urn:nbn:se:hj:diva-62484 (URN)10.1016/j.msea.2023.145618 (DOI)001087353900001 ()2-s2.0-85169977535 (Scopus ID)HOA;intsam;905111 (Local ID)HOA;intsam;905111 (Archive number)HOA;intsam;905111 (OAI)
Available from: 2023-09-19 Created: 2023-09-19 Last updated: 2025-10-13Bibliographically approved

Open Access in DiVA

Kappa(11556 kB)1807 downloads
File information
File name FULLTEXT01.pdfFile size 11556 kBChecksum SHA-512
4afdb38804f4998c9bedc80125be7a856c62dac62664f4f768065e756e5e2a7c266b349f27e23e56424400d847824df6b9795727d13758739498486fb2eaa3db
Type fulltextMimetype application/pdf

Authority records

Bogdanoff, Toni

Search in DiVA

By author/editor
Bogdanoff, Toni
By organisation
JTH, Materials and Manufacturing
Metallurgy and Metallic Materials

Search outside of DiVA

GoogleGoogle Scholar
Total: 1820 downloads
The number of downloads is the sum of all downloads of full texts. It may include eg previous versions that are now no longer available

isbn
urn-nbn

Altmetric score

isbn
urn-nbn
Total: 1366 hits
CiteExportLink to record
Permanent link

Direct link
Cite
Citation style
  • apa
  • ieee
  • modern-language-association-8th-edition
  • vancouver
  • Other style
More styles
Language
  • de-DE
  • en-GB
  • en-US
  • fi-FI
  • nn-NO
  • nn-NB
  • sv-SE
  • Other locale
More languages
Output format
  • html
  • text
  • asciidoc
  • rtf